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《中藥白附子和娑羅子的化學(xué)成分研究及白附子腦苷a的全合成-生藥學(xué)專(zhuān)業(yè)畢業(yè)論文》由會(huì)員上傳分享,免費(fèi)在線(xiàn)閱讀,更多相關(guān)內(nèi)容在學(xué)術(shù)論文-天天文庫(kù)。
1、ListofabbreviationsCI.MSChemicalIonizationMassSpectrumCOSYCorrelationSpectroscopyDBU1,8-Diazabicyclo[5,4,O]undec一7一eneDCCDicyclohexyIcarbodiimideD.GalD—galactoseD—GIuD—glucoseD1BAL—HDiisobut,rlaluminiumhydrideDMAP4一N.N—dimethylaminopyridineDMFN,N—dimethylfo
2、rmamideEI—MSElectronImpactMassSpectrumESI.MSElectronSprayIonizationMassSpectrumFABMSFastAtomBombardmentSourceHMBCHeteronuclearMultipleBondConnectivityby2DMultiple—quantumCoherenceHMPAHexamethylphosphoramideHMQC1H—DetectedHeteronuclearMultiple—QuantumCoheren
3、ceviaDirectCouplingHOBt1一HydroxybenzotriazoleHPLCHighPerformanceLiquidChromatographyHR—MSHighResolutionMassSpectrumIRInfraredNMRNuclearMagneticResonancePDCPyridiniumDichromatePrepHPLCPreparativeHighPerformanceLiquidChro——matographyP。T§OHP—Toluenesulfonicaci
4、dRtRetentiontimeSI.MSSecondaryIonMassSpectrumTLCThinLayerChromatographyTrClTriphenylmethylchorideTOF.MSTimeofFlyingMassSpectrumListofTablesTable1.1SomespeciesofTyphoniumgenususedas17drugsandherbaldrugsinChinaTable1-2Somecerebrosidesfoundinnaturalresources24
5、Table1-3Somecatalystusedintheacylatingreaction34Table1—4Someglycosyl.groupsusedintheglycosidation35Table2-1TheConstituentsisolatedfromTyphonium43giganteumEn91.Table2-2NMRdataforTyphonosideA(1)(500MHzfor521Hand125MHzfor13CNMRinCsDsN)Table2-3NMRdataforTyphono
6、sideB(2)(500MHzfor541Hand125MHzfor”CNMRinC5D5N)Table2.4NMRdataforTyphonosideC(9)(500MHzfor561Hand125MHzfor13CNMRinC5D5N)Table2-5NMRdataforTyphonosideD(10)(500MHzfor611Hand125MHzfor13CNMRinC5D5N)Table2-6Theresultsofsomechemicalconstituents63experimentsTable2
7、-7TheconstituentsseparatedbyPrep—HPLC693Table2—8Thetypesofsomecerebrosidestructures8lTable2.9Theexperimentofanti—bloodcoagulation,90viscosityofbloodandplasmaviscosity(Tweenasthereference)Table2.10TheexperimentforT901l—lAofanti—blood90coagulmion,viscosityofb
8、loodandplasmaviscosityTable2-11TheexperimentforX9004··3ofanti·-blood91coagulation,viscosityofbloodandplasmaviscosityTable2-12TheexperimentsforT9004—3,T901卜IAon91bloodviscosityTable2-13TheexperimentforT