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1、METHOD8261VOLATILEORGANICCOMPOUNDSBYVACUUMDISTILLATIONINCOMBINATIONWITHGASCHROMATOGRAPHY/MASSSPECTROMETRY(VD/GC/MS)1.0SCOPEANDAPPLICATION1.1Method8261isusedtodeterminetheconcentrationsofvolatileorganiccompounds,andsomelow-boilingsemivolatileorganiccompounds,inavarietyof
2、liquid,solid,andoilywastematrices,aswellasanimaltissues.Thismethodisapplicabletonearlyalltypesofmatricesregardlessofwater,soil,sediment,sludge,oil,andbiotacontent.Method8261isusefulinthedeterminationofthefollowingcompounds:CompoundCASRegistryNo.Acetone67-64-1Acetonitril
3、e75-05-8Acetophenone98-86-2Acrolein107-02-8Acrylonitrile107-13-1AllylChloride107-05-1Aniline62-53-3Benzene71-43-2Bromochloromethane75-97-5Bromodichloromethane75-27-4Bromoform75-25-2Bromomethane74-83-92-Butanone78-93-3n-Butylbenzene104-51-8sec-Butylbenzene135-98-8tert-Bu
4、tylbenzene98-06-6Carbondisulfide75-15-0Carbontetrachloride56-23-5Chlorobenzene108-90-7Chlorodibromomethane124-48-1Chloroethane75-00-3Chloroform67-66-3Chloromethane74-87-32-Chlorotoluene95-49-84-Chlorotoluene106-43-41,2-Dibromo-3-chloropropane96-12-88261-1Revision0Novemb
5、er2000CompoundCASRegistryNo.Dibromomethane74-95-31,2-Dichlorobenzene95-50-11,3-Dichlorobenzene541-73-11,4-Dichlorobenzene106-46-7cis-1,4-Dichloro-2-butene764-41-0trans-1,4-Dichloro-2-butene110-57-6Dichlorodifluoromethane75-71-81,1-Dichloroethane75-35-41,2-Dichloroethane
6、107-06-21,1-Dichloroethene75-35-3trans-1,2-Dichloroethene156-60-5cis-1,2-Dichloroethene156-59-21,2-Dichloropropane78-87-51,3-Dichloropropane142-28-92,2-Dichloropropane594-20-71,1-Dichloropropene563-58-6cis-1,3-Dichloropropene10061-01-5trans-1,3-Dichloropropene10061-02-6
7、Diethylether60-29-71,4-Dioxane128-91-1Ethylacetate141-78-6Ethylbenzene100-41-4Ethylmethacrylate97-63-2Hexachlorobutadiene87-68-32-Hexanone591-78-6Iodomethane74-88-4Isobutylalcohol78-83-1Isopropylbenzene98-82-8p-Isopropyltoluene99-87-6Methacrylonitrile126-98-7Methylenech
8、loride75-09-2Methylmethacrylate80-62-61-Methylnaphthalene90-12-02-Methylnaphthalene91-57-64-Methyl-2-pentanone