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1、催化劑裝量60ml,不同空速條件下的反應(yīng)結(jié)果:實(shí)際反應(yīng)溫度623°C623°C624°C624°C624°C平均CH4C2H6C2H4C3H8C3H6C43.163.291.1247.7443.361.332.7841.1948.4842.271.272.94.121.2449.341.071.343.014.111.1550.3440.011.393.044.041.1351.6538.671.472.9783.9121.16649.50241.0761.36應(yīng)溫度CH4C2H6C2H4C3H8C3H6C4602°C2.492.210.754.7638.141.
2、7602°C2.032.630.6654.438.881.41602°C1.932.690.6855.1538.021.53604°C1.912.70.6555.4137.71.63605°C1.922.780.7355.3737.541.66平均2.0562.6020.68455.01838.0561.586:.休積空速1000,（折算成質(zhì)量空速是1.86,；流化速度0.16m/s）實(shí)際反應(yīng)溫度CH4C2H6C2H4C3H8C3H6C4603°C2.581.820.8455.8236.931.93599°C1.612.240.5155.3838.481.7959
3、9°C1.72.590.7655.4437.371.66603°C1.742.660.7756.1736.461.71603°C1.732.580.7257.2835.871.81平均1.8722.3780.7256.01837.0221.78體積空速1200,（折算成質(zhì)量空速是2.23,流化速度0.20m/s）實(shí)際反應(yīng)溫度CH4C2H6C2H4C3H8C3H6C4604°C2.061.550.757.2136.511.98599°C1.361.890.4856.6537.781.85599°C1.42.10.6458.1335.841.88600°C1.512.
4、210.675&335.481.83601°C1.512.160.658.6435.12平均1.5681.9820.61857.78636.1421.908木實(shí)驗(yàn)采用固定流化床反應(yīng)器，反應(yīng)段直徑20儷,原料氣體組成為丙烷占93.17%,丙烯3.17%,C4占3.66%,催化劑密度為1.06g/ml，試驗(yàn)結(jié)果按照質(zhì)量分?jǐn)?shù)計(jì)算,催化劑連續(xù)反應(yīng)一小時(shí)左右，采用氣相色譜在線分析，每十分鐘取樣一次。一以下是在設(shè)定反應(yīng)溫度為620°C,催化劑裝量為60ml,不同空速條件下的反應(yīng)結(jié)果：1.體積空速800,（折算成質(zhì)量空速是1.49,流化速度0.13m/s）二以下是設(shè)定反應(yīng)溫度為
5、640°C,4.體積空速800,（折算成質(zhì)量空速是1.49,流化速度0.13m/s）5.體積空速1000,（折算成質(zhì)量空速是1.86,流化速度0.17m/s）實(shí)際反CH4C2H6C2H4C3H8C3H6C4應(yīng)溫度625°C2.252.341.0551.5240.782.06622°C2.062.790.8450.9541.041.44624°C2.53.490.9850.0541.561.41621°C1.762.080.9557.4835.492.18622°C1.82.230.8956.8136.062.16平均2.0742.5860.94253.36238.
6、9861.85..設(shè)定溫度640°C,體積空速1200,（折算成質(zhì)量空速是2.23,流化速度0.20m/s）實(shí)際反應(yīng)溫度CH4C2H6C2H4C3H8C3H6C4620°C1.641.580.7856.4537.272.29618°C1.371.790.6455.8838.192.13618°C1.682.160.7955.5237.871.92619°C1.82.320.8755.7637.132.05620°C1.762.290.8456.7736.232.07平均1.652.0280.78456.07637.3382.092三以下是設(shè)定反應(yīng)溫度為620°C,
7、原料氣體流量為0.084m3/h（流化速度0.23m/s），在不同催化劑裝量條件下的反應(yīng)結(jié)果：7.催化劑裝量70ml,（折算成體積空速1200,質(zhì)量空速2.23）應(yīng)溫度CH4C2H6C2H4C3H8C3H6C4593°C2.061.20.561.631.942.71587°C1.431.910.3660.3333.842.13587°C1.482.270.7960.432.892.11588°C1.462.271.0860.1732.72.29589°C1.4220.4261.3332.552.27平均1.571.930.6360.76632.7842.3028.
8、催化劑裝量
