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1、INORGANICSYNTHESESVolumeXXI.....................*.....................BoardofDirectorsHENRYF.HOLTZCLAWUniversityofNebruskuJAYH.WORRELLUniversityofSouthFloridaBODlEE.DOUGLASUniversityofPittsbuurghDUWARDF.SHRIVERNorthwesternUniversityDARYLEH.BUSCHOhioStute
2、UniversityFutureVolumesXXIISMITHL.HOLTOklahomaStateUniversityXXIIISTANLEYKIRSCHNERWuyneStuteUniversityXXIVJEAN'NEM.SHREEVEUniversityofIduhoXXVHERBERTD.KAESZUniversityofCuliforniu,LosAngelesInternationalAssociatesE.0.FISCHERTechnischeUniversitatMunichJACK
3、LEWISCambridgeUniversityLAMBERTOMALATESTAUniversityofMilunF.G.A.STONEUniversftyofBristolGEOFFREYWILKINSONImperiulCollegeofScienceundTechnologyLondonAKIOYAMAMOTOTokyoInstituteofTechnologyYokohamuMARTINA.BENNETTAustruliunNutionulUniversityR.POILBLANCNation
4、01CenterforScientifcResearchToulouseH.W.ROESKYUniversityGottingenEditor-inChiefJOHNP.FACKLER,JR.DepartmentofChemistry....................CaseWesternReserveUniversity.......................INORGANICSYNTHESESVolumeXXIAWiley-IntersciencePublicationJOHNWILEY
5、&SONSNewYorkChichesterBrisbaneTorontoSingaporePublishedbyJohnWiley&Sons,Inc.Copyright01982InorganicSyntheses,Inc.Allrightsreserved.PublishedsimultaneouslyinCanada.ReproductionortranslationofanypartofthisworkbeyondthatpermittedbySection107or108ofthe1976Un
6、itedStatesCopyrightActwithoutthepermissionofthecopyrightownerisunlawful.RequestsforpermissionorfurtherinformationshouldbeaddressedtothePermissionsDepartment,JohnWiley&Sons,Inc.LibraryofCongressCatalogNumber:39-23015ISBN0-471-86520-6PrintedintheUnitedStat
7、esofAmerica10987654321PREFACEInorganicSynthesescontinuestofulfillavitalroleforinorganicchemistsandotherusersofinorganicandorganometallicmaterials.Twentyvolumesand42yearshaveelapsedsinceHaroldS.Bootheditedthefirstvolumeintheseries.WhileIdidnothavetheoppor
8、tunitytoknowBooth,hisghostoccasionallyreturnstothesehallsatCaseWesternReserveUniversitytoremindusofthegreatforwardstridesInorganicChemistryhasmadesinceWorldWar11.Whowouldhaveknownthenthatchromousacetate(InorganicSyntheses,
