資源描述：
《取代吲哚-3-甲醛芳香腙類化合物的合成》由會(huì)員上傳分享，免費(fèi)在線閱讀，更多相關(guān)內(nèi)容在學(xué)術(shù)論文-天天文庫(kù)。
1、2007東南大學(xué)碩士學(xué)位論文摘要由取代吲哚一3一甲醛和各種取代苯肼或取代苯肼鹽酸鹽在酸性條件下通過(guò)縮合反應(yīng)生成一系列取代吲哚一3一甲醛芳香腙類化合物。本文共合成了19個(gè)新的取代吲哚一3一甲醛芳香腙類化合物：4一甲氧羰基吲哚-3-甲醛苯腙、5一甲氧羰基吲哚一3一甲醛苯腙、6一甲氧羰基吲哚一3一甲醛苯腙、7一甲氧羰基吲哚一3一甲醛苯腙；4一氰基吲哚一3一甲醛苯腙、5一氰基吲哚一3一甲醛苯腙、6一氰基吲哚一3一甲醛苯腙；4一氰基吲哚一3一甲醛對(duì)甲苯腙、5一氰基吲哚一3一甲醛對(duì)甲苯腙、6一氰基吲哚一3一甲醛對(duì)甲苯腙；4一
2、氰基吲哚一3一甲醛對(duì)硝基苯腙、5一氰基吲哚一3一甲醛對(duì)硝基苯腙、6一氰基吲哚一3一甲醛對(duì)硝基苯腙；5-芐氧基吲哚一3一甲醛對(duì)甲苯腙、6一芐氧基吲哚一3一甲醛對(duì)甲苯腙、7一芐氧基吲哚一3一甲醛對(duì)甲苯腙；5一甲氧基吲哚-3-甲醛對(duì)甲苯腙、6一甲氧基吲哚一3一甲醛對(duì)甲苯腙；6一氯吲哚一3一甲醛對(duì)甲苯腙。該19個(gè)化合物均未見(jiàn)文獻(xiàn)報(bào)道。這些化合物的結(jié)構(gòu)均經(jīng)IR、1剛豫、Ms得到確證，并獲得了熔點(diǎn)等相關(guān)物理數(shù)據(jù)。關(guān)鍵詞：取代吲哚一3一甲醛芳香腙，取代吲哚一3一甲醛，縮合反應(yīng)，合成2007東南大學(xué)碩士學(xué)位論文AbstractA
3、seriesofsubstitutedindole一3一carboxaldehydephenylhydrazonesw91"esynthesizedbycondensationreactionwithsubstitutedindole一3一carboxaldehydesandsubstitutedphenylhydrazinesinacidcondition．Nineteenne、】lrcompounds，substitutedindole-3一carboxaldehydephenylhydrazones．hav
4、ebeensynthesizcd．Theyare4一methoxycarbonylindole-3一carboxaldehydephenylh-ydrazone，5-methoxycarbonylindole-3一carboxaldehydephenylhydrazone，6-methoxyc—arbonylindole一3一carboxaldehydephenylhydrazone，7-methoxycarbonylindole-3一carbo—xaldehydephenylhydrazone，4-cyanoi
5、ndole一3一carboxaldehydephenylhydrazone，5-cya—noindole一3一carboxaldehydephenyllaydrazone，6-cyanoindole一3一carboxaldehydepheny—lhydrazone．4一cyanoindole·3一carboxaldehyde-p-methylphenylhydrazone,5-cyanoi—ndole一3一carboxaldehyde-P—methylphenylhydrazone,6-cyanoindole．3
6、．carboxaide-hyde·P—methylphenylhydrazone，4-cyanoindole一3一carboxaldehyde-p—nitrophenyl·hydrazone，5-cyanoindole-3·carboxaldehyde-p·nitrophenylhydrazone,6-cyanoindole·3-carboxaldehyde-P．nitrophenylhydrazone．5-benzyloxyindole．3．carboxaldehyde-p·methylphenylhydraz
7、one，6-benzyloxy-indole一3一carboxaldehyde-p-methylphenylhydrazone,7-benzyloxyindole-3一carboxaldehyde—P-methylphenylhydrazone，5-methoxyindole一3一carboxaldehyde-p．methylphenylhydrazone．6一methoxy-indole一3一carboxald·ehyde-p-methylphenylhydrazone．6-chloroindole·3一car
8、boxaldehyde—p-methylphenylhydrazone．Thesecompoundshaveallnotbeenreported．AncompoundswereconfirmedbyIR．HNMRandMS．Andsomephysicalpropertieshavebeenfoundatthesametime．Keywords：substitutedind
