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1、中文摘要本實(shí)驗(yàn)利用掃描電子顯微鏡、金剛石單顆??箟簭?qiáng)度測定儀等測試設(shè)備,系統(tǒng)地研究了在陶瓷剛玉磨料的制備過程中原料的初始濃度、氨水的加入方式、球磨時(shí)間、添加劑的成分、配比和加入量、燒結(jié)溫度對磨料的顯微結(jié)構(gòu)、單顆??箟簭?qiáng)度的影響。實(shí)驗(yàn)結(jié)果表明,原料的初始濃度、氨水的加入方式、球磨時(shí)間、添加劑的成分、配比、加入量、燒結(jié)溫度對磨料的性能均有很大的影響。磨料的晶粒尺寸隨原料初始濃度的升高而增大,而單顆粒抗壓強(qiáng)度則隨原料初始濃度的升高而降低;氨水加入速度過快導(dǎo)致磨料的晶粒尺寸變大,致密性變差,單顆??箟簭?qiáng)度下降;球磨時(shí)間并非越長越好,采用合理的球磨時(shí)問,既能提
2、高磨料性能,又能提高生產(chǎn)效率;選取合適的添加劑成分能有效地控制晶粒的大小,提高磨料的致密性;適當(dāng)?shù)奶砑觿┡浔炔坏梢杂行У卮龠M(jìn)氧化鋁燒結(jié),抑止晶粒的長大,同時(shí)可以提高磨料的單顆??箟簭?qiáng)度;加入適量的添加劑能夠細(xì)化晶粒,提高磨料的單顆??箟簭?qiáng)度;燒結(jié)溫度對磨料的性能影響較為明顯,采用合適的燒結(jié)溫度才能得到較佳性能的氧化鋁磨料。關(guān)鍵詞:陶瓷剛玉,磨料,制備工藝,性能ABSTRACTInthepreparationprocessofceramiccorundumabrasives,theeffectsoftheinitialconcentrationofr
3、awmaterials,theaddingmethodsoftheammonia,ballmillingtime,differentadditivesandtheircomposition,additionamountandsinteringtemperatureonthemicrostructure,singleparticlecompressivestrengthoftheabrasivesw.ereresearchedsystematicallyviascanningelectronicmicroscope(SEMlanddiamondsing
4、leparticlecompressivestrengthtester.Theresultsshowedthatthepropertiesoftheabrasiveswereinfluencedremarkablybytheinitialconcentrationofthematerials,theballmillingtime,theaddingmethodsofammonia,additivesandtheircomposition,additionamountandsinteringtemperature.Withtheincreaseofth
5、einitialconcentrationofrawmaterials,thegrainsizeofabrasivesincreased,buttheabrasive’Ssingleparticlecompressivestrengthreduced.Theexcessiveaddingspeedoftheammoniawouldinducetherapidgrowthofabrasivegrains,thepoorcompactnessoftheabrasivesandthedeclineofsingleparticlecompressivestr
6、ength.Longerballmillingtimedidn’tconsequentiallyresultinbeRerpropertiesofabrasives,properballmillingtimewouldnotonlyimprovethepropertiesofabrasives,butincreasetheproductionefficiency.Thegrainsizecouldbecontrolledeffectivelyandthecompactnessoftheabrasiveswouldbeimprovedgreatlyby
7、choosingsuitableadditives.Properadditivescompositionwouldpromotethesinteringofalumina,restrainthegrowthofgrainsandimprovethesingleparticlecompressivestrengthofabrasives.Thegrainscouldbefreedandthesingleparticlecompressivestrengthofabrasivescouldbeincreasedbyaddingappropriateamo
8、untofadditives.Sinteringtemperaturehadobviouseffectont